Authors: W. Zhang and A. Chatt 1
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  • 1 Dalhousie University SLOWPOKE-2 Reactor Facility, Trace Analysis Research Centre, Department of Chemistry Halifax NS B3H 4J3 Canada
  • | 2 Radiation Protection Bureau of Health Canada 775 Brookfield Road, AL 6302D1 Ottawa ON K1A 1C1 Canada
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Abstract  

A pseudo-cyclic instrumental neutron activation analysis method in conjunction with anti-coincidence gamma-ray spectrometry (PC-INAA-AC) has been developed for the determination of ppb levels of Se. The method consists of repetitions of the irradiation-decay-counting cycles of a sample using the rapid transfer cyclic system at the Dalhousie University SLOWPOKE-2 reactor facility. The 162-keV γ-ray of 77mSe (t1/2 = 17.4 s) has been found to be highly selective. The precision and detection limits are significantly improved and the total experimental time drastically reduced by this method. Detection limits are between 2 and 9 ng. The accuracy of the method has been evaluated by analyzing a number of nutritional reference materials. The PC-INAA-AC method has been applied for the routine determination of Se to the composites of 135 food samples with values ranging from as low as 1 ng g−1 for tea to 1,045 ng g−1 for organ meats on fresh weight basis.

Manuscript Submission: HERE

  • Impact Factor (2019): 1.137
  • Scimago Journal Rank (2019): 0.360
  • SJR Hirsch-Index (2019): 65
  • SJR Quartile Score (2019): Q3 Analytical Chemistry
  • SJR Quartile Score (2019): Q3 Health, Toxicology and Mutagenesis
  • SJR Quartile Score (2019): Q2 Nuclear Energy and Engineering
  • SJR Quartile Score (2019): Q3 Pollution
  • SJR Quartile Score (2019): Q3 Public Health, Environmental and Occupational Health
  • SJR Quartile Score (2019): Q3 Radiology, Nuclear Medicine and Imaging
  • SJR Quartile Score (2019): Q3 Spectroscopy
  • Impact Factor (2018): 1.186
  • Scimago Journal Rank (2018): 0.408
  • SJR Hirsch-Index (2018): 60
  • SJR Quartile Score (2018): Q2 Nuclear Energy and Engineering
  • SJR Quartile Score (2018): Q2 Pollution

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Journal of Radionalytical and Nuclear Chemistry
Language English
Size A4
Year of
Foundation
1968
Volumes
per Year
4
Issues
per Year
12
Founder Akadémiai Kiadó
Founder's
Address
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
Publisher Akadémiai Kiadó
Springer Nature Switzerland AG
Publisher's
Address
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
CH-6330 Cham, Switzerland Gewerbestrasse 11.
Responsible
Publisher
Chief Executive Officer, Akadémiai Kiadó
ISSN 0236-5731 (Print)
ISSN 1588-2780 (Online)