Summary
This paper describes a simple, precise, and accurate HPTLC method for simultaneous quantification of sennoside A, sennoside B, and kaempferol in Cassia fistula whole plant extract. Chromatographic separation of the sample extract was performed on aluminium foil plates coated with silica gel 60 F254 as stationary phase. The mobile phase was toluene-ethyl acetate-methanol-formic acid 8:10:5:2 (υ/υ). Densitometric evaluation of the separated bands was performed at 270 nm. Sennosides A and B and kaempferol were satisfactorily resolved at RF 0.22 ± 0.05, 0.19 ± 0.05, and 0.81 ± 0.05, respectively. Recovery of sennosides A and B and kaempferol from Cassia fistula extract was 98.03, 98.74, and 99.08%, respectively. The method was validated for specificity, accuracy, linearity (100–400 ng per band), and precision (instrument precision in the range 1.03–1.33 and method precision in the range of 1.31–1.75) in accordance with ICH guidelines.
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Senior editors
Editor(s)-in-Chief: Kowalska, Teresa (1946-2023)
Editor(s)-in-Chief: Sajewicz, Mieczyslaw
Editors(s)
- Danica Agbaba (University of Belgrade, Belgrade, Serbia)
- Łukasz Komsta (Medical University of Lublin, Lublin, Poland)
- Ivana Stanimirova-Daszykowska (University of Silesia, Katowice, Poland)
- Monika Waksmundzka-Hajnos (Medical University of Lublin, Lublin, Poland)
Editorial Board
- R. Bhushan (The Indian Institute of Technology, Roorkee, India)
- J. Bojarski (Jagiellonian University, Kraków, Poland)
- B. Chankvetadze (State University of Tbilisi, Tbilisi, Georgia)
- M. Daszykowski (University of Silesia, Katowice, Poland)
- T.H. Dzido (Medical University of Lublin, Lublin, Poland)
- A. Felinger (University of Pécs, Pécs, Hungary)
- K. Glowniak (Medical University of Lublin, Lublin, Poland)
- B. Glód (Siedlce University of Natural Sciences and Humanities, Siedlce, Poland)
- A. Gumieniczek (Medical University of Lublin, Lublin, Poland)
- U. Hubicka (Jagiellonian University, Kraków, Poland)
- K. Kaczmarski (Rzeszow University of Technology, Rzeszów, Poland)
- H. Kalász (Semmelweis University, Budapest, Hungary)
- K. Karljiković Rajić (University of Belgrade, Belgrade, Serbia)
- I. Klebovich (Semmelweis University, Budapest, Hungary)
- A. Koch (Private Pharmacy, Hamburg, Germany)
- P. Kus (Univerity of Silesia, Katowice, Poland)
- D. Mangelings (Free University of Brussels, Brussels, Belgium)
- E. Mincsovics (Corvinus University of Budapest, Budapest, Hungary)
- Á. M. Móricz (Centre for Agricultural Research, Budapest, Hungary)
- G. Morlock (Giessen University, Giessen, Germany)
- A. Petruczynik (Medical University of Lublin, Lublin, Poland)
- R. Skibiński (Medical University of Lublin, Lublin, Poland)
- B. Spangenberg (Offenburg University of Applied Sciences, Germany)
- T. Tuzimski (Medical University of Lublin, Lublin, Poland)
- Y. Vander Heyden (Free University of Brussels, Brussels, Belgium)
- A. Voelkel (Poznań University of Technology, Poznań, Poland)
- B. Walczak (University of Silesia, Katowice, Poland)
- W. Wasiak (Adam Mickiewicz University, Poznań, Poland)
- I.G. Zenkevich (St. Petersburg State University, St. Petersburg, Russian Federation)
KOWALSKA, TERESA (1946-2023)
E-mail: kowalska@us.edu.pl
SAJEWICZ, MIECZYSLAW
E-mail:msajewic@us.edu.pl
Indexing and Abstracting Services:
- Science Citation Index
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- Chemical and Earth Sciences
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- CABI
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| 2021 | |
|---|---|
| Web of Science | |
| Total Cites WoS |
652 |
| Journal Impact Factor | 2,011 |
| Rank by Impact Factor | Chemistry, Analytical 66/87 |
| Impact Factor without Journal Self Cites |
1,789 |
| 5 Year Impact Factor |
1,350 |
| Journal Citation Indicator | 0,40 |
| Rank by Journal Citation Indicator | Chemistry, Analytical 72/99 |
| Scimago | |
| Scimago H-index |
29 |
| Scimago Journal Rank |
0,27 |
| Scimago Quartile Score | Chemistry (miscellaneous) (Q3) |
| Scopus | |
| Scopus Cite Score |
2,8 |
| Scopus CIte Score Rank |
General Chemistry 210/409 (Q3) |
| Scopus SNIP |
0,586 |
|
2020
|
|
|
Total Cites
|
650
|
|
WoS
|
|
|
Journal
Impact Factor |
1,639
|
|
Rank by
|
Chemistry, Analytical 71/83 (Q4)
|
|
Impact Factor
|
|
|
Impact Factor
|
1,412
|
|
without
|
|
|
Journal Self Cites
|
|
|
5 Year
|
1,301
|
|
Impact Factor
|
|
|
Journal
|
0,34
|
|
Citation Indicator
|
|
|
Rank by Journal
|
Chemistry, Analytical 75/93 (Q4)
|
|
Citation Indicator
|
|
|
Citable
|
45
|
|
Items
|
|
|
Total
|
43
|
|
Articles
|
|
|
Total
|
2
|
|
Reviews
|
|
|
Scimago
|
28
|
|
H-index
|
|
|
Scimago
|
0,316
|
|
Journal Rank
|
|
|
Scimago
|
Chemistry (miscellaneous) Q3
|
|
Quartile Score
|
|
|
Scopus
|
393/181=2,2
|
|
Scite Score
|
|
|
Scopus
|
General Chemistry 215/398 (Q3)
|
|
Scite Score Rank
|
|
|
Scopus
|
0,560
|
|
SNIP
|
|
|
Days from
|
58
|
|
submission
|
|
|
to acceptance
|
|
|
Days from
|
68
|
|
acceptance
|
|
|
to publication
|
|
|
Acceptance
|
51%
|
| Rate |
| 2019 | |
|---|---|
| Total Cites WoS |
495 |
| Impact Factor | 1,418 |
| Impact Factor without Journal Self Cites |
1,374 |
| 5 Year Impact Factor |
0,936 |
| Immediacy Index |
0,460 |
| Citable Items |
50 |
| Total Articles |
50 |
| Total Reviews |
0 |
| Cited Half-Life |
6,2 |
| Citing Half-Life |
8,3 |
| Eigenfactor Score |
0,00048 |
| Article Influence Score |
0,164 |
| % Articles in Citable Items |
100,00 |
| Normalized Eigenfactor |
0,05895 |
| Average IF Percentile |
20,349 |
| Scimago H-index |
26 |
| Scimago Journal Rank |
0,255 |
| Scopus Scite Score |
226/167=1,4 |
| Scopus Scite Score Rank |
Chemistry (miscellaneous) 240/398 (Q3) |
| Scopus SNIP |
0,494 |
| Acceptance Rate |
41% |
| Acta Chromatographica | |
|---|---|
| Publication Model | Online only Gold Open Access |
| Submission Fee | none |
| Article Processing Charge | 400 EUR/article |
| Regional discounts on country of the funding agency | World Bank Lower-middle-income economies: 50% World Bank Low-income economies: 100% |
| Further Discounts | Editorial Board / Advisory Board members: 50% Corresponding authors, affiliated to an EISZ member institution subscribing to the journal package of Akadémiai Kiadó: 100% |
| Subscription Information | Gold Open Access |
| Purchase per Title | |
| Acta Chromatographica | |
|---|---|
| Language | English |
| Size | A4 |
| Year of Foundation |
1988 |
| Volumes per Year |
1 |
| Issues per Year |
4 |
| Founder | Institute of Chemistry, University of Silesia |
| Founder's Address |
PL-40-007 Katowice, Poland, Bankowa 12 |
| Publisher | Akadémiai Kiadó |
| Publisher's Address |
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245. |
| Responsible Publisher |
Chief Executive Officer, Akadémiai Kiadó |
| ISSN | 2083-5736 (Online) |
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| Abstract Views | Full Text Views | PDF Downloads | |
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| Dec 2022 | 0 | 10 | 7 |
| Jan 2023 | 0 | 10 | 7 |
| Feb 2023 | 0 | 0 | 5 |
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| Apr 2023 | 0 | 2 | 1 |
| May 2023 | 0 | 5 | 4 |
| Jun 2023 | 0 | 1 | 2 |
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