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Alastair BakerCardiff University, Park Place, Main Building, Cardiff CF10 3AT, UK

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Michael GrazWillowbrook Technical Units, Llandogo Road, St. Mellons, Cardiff CF3 0EF, UK

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Robert SaundersWillowbrook Technical Units, Llandogo Road, St. Mellons, Cardiff CF3 0EF, UK

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Gareth J. S. EvansWillowbrook Technical Units, Llandogo Road, St. Mellons, Cardiff CF3 0EF, UK

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Ilaria PitottiCardiff University, Park Place, Main Building, Cardiff CF10 3AT, UK

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Thomas WirthCardiff University, Park Place, Main Building, Cardiff CF10 3AT, UK

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Rapid alkylations of thiols are performed in a packed-bed flow reactor where potassium carbonate acts as a heterogeneous base in anhydrous solvents at ambient temperature. The reaction also has a high efficiency as the removal of the solvent is the only work up required to isolate the product. The products can be used in a subsequent oxidation which was performed sequentially in semibatch mode. The alkylations of phenol and benzyl amine have been demonstrated on an array of bases, but higher temperatures and longer reaction times are required than with thiols.

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Journal of Flow Chemistry
Language English
Size A4
Year of
Foundation
2011
Volumes
per Year
1
Issues
per Year
4
Founder Áramlásos Kémiai Tudományos Társaság
Founder's
Address
H-1031 Budapest, Hungary Záhony utca 7.
Publisher Akadémiai Kiadó
Springer Nature Switzerland AG
Publisher's
Address
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
CH-6330 Cham, Switzerland Gewerbestrasse 11
Responsible
Publisher
Chief Executive Officer, Akadémiai Kiadó
ISSN 2062-249X (Print)
ISSN 2063-0212 (Online)

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